(1alpha,2beta,5alpha)-2-methyl-5-(1-methylethyl)bicyclo[3.1.0]hexan-2-ol

  • Name: (1alpha,2beta,5alpha)-2-methyl-5-(1-methylethyl)bicyclo[3.1.0]hexan-2-ol
  • CAS: 15537-55-0
  • Purity: 99%
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Details

Manufacturer supply top purity (1alpha,2beta,5alpha)-2-methyl-5-(1-methylethyl)bicyclo[3.1.0]hexan-2-ol 15537-55-0 with GMP standards

  • Molecular Formula: C10H18O
  • Molecular Weight: 154.252
  • Melting Point: 36.5-37.2 °C 
  • Boiling Point: 201.7°Cat760mmHg 
  • PKA: 15.22±0.40(Predicted) 
  • Flash Point: 80.1°C 
  • PSA： 20.23000 
  • Density: 1.03g/cm3 
  • LogP: 2.19350 

15537-55-0 Relevant articles

Cyclopropanation with dibromomethane under grignard and barbier conditions

Brunner, Gerhard,Eberhard, Laura,Oetiker, Juerg,Schroeder, Fridtjof

scheme or table, p. 3708 - 3718 (2010/04/02)

Tertiary Grignard reagents and dibromome...

Tandem cyclopropanation with dibromomethane under Grignard conditions

Brunner, Gerhard,Eberhard, Laura,Oetiker, Juerg,Schroeder, Fridtjof

, p. 7543 - 7554 (2008/12/22)

(Chemical Equation Presented) Tertiary G...

Allylic Lithium Oxyanionic Directed and Facilitated Simmons-Smith Cyclopropanation: Stereoselective Synthesis of (±)-cis-Sabinene Hydrate and a Novel Ring Expansion

Cheng, Dai,Kreethadumrongdat, Thanapong,Cohen, Theodore

, p. 2121 - 2123 (2007/10/03)

(matrix presented) The lithium salts of ...

A short and efficient synthesis of (±)-trans-sabinene hydrate

Galopin, Christophe C.

, p. 5589 - 5591 (2007/10/03)

A short synthesis of sabinene hydrate is...

15537-55-0 Process route

1-isopropenyl-4-methylbicyclo[3.1.0]hexan-4-ol

1-isopropenyl-4-methylbicyclo[3.1.0]hexan-4-ol

1-isopropyl-4-methylbicyclo[3.1.0]hexan-4-ol
546-79-2,3484-42-2,5157-77-7,7712-82-5,15537-55-0,15826-82-1,15826-83-2,17699-16-0,58117-61-6,117305-49-4

1-isopropyl-4-methylbicyclo[3.1.0]hexan-4-ol

Conditions
Conditions Yield
With copper diacetate; dihydrogen peroxide; hydrazine hydrate; In ethanol; at 0 - 20 ℃;
63%
With hydrogen; platinum barium sulfate;
diiodomethane
75-11-6

diiodomethane

3-isopropyl-cyclopent-2-enone
1619-28-9

3-isopropyl-cyclopent-2-enone

methyllithium
917-54-4

methyllithium

1-isopropyl-4-methylbicyclo[3.1.0]hexan-4-ol
546-79-2,3484-42-2,5157-77-7,7712-82-5,15537-55-0,15826-82-1,15826-83-2,17699-16-0,58117-61-6,117305-49-4

1-isopropyl-4-methylbicyclo[3.1.0]hexan-4-ol

Conditions
Conditions Yield
3-isopropyl-cyclopent-2-enone; methyllithium; In diethyl ether; at -78 - 0 ℃;
diiodomethane; With iodine; copper; zinc; In diethyl ether; for 2h; Further stages.; Heating;
64%

15537-55-0 Upstream products

  • 917-54-4
    917-54-4

    methyllithium

  • 75-11-6
    75-11-6

    diiodomethane

  • 1619-28-9
    1619-28-9

    3-isopropyl-cyclopent-2-enone

  • 68677-08-7
    68677-08-7

    epoxisabinene

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